employed
a thermite process by which a zirconium salt was reduced by aluminium
at high temperatures in vacuum, and in order to avoid contamination
of the metal by the residual gases in an Arsem carbon furnace Burch
suggested heating the metal by eddy currents. Thus the Company came
to make the first vacuum high-frequency induction furnace, and the
final design incorporated the first water-cooled anode valve to be
used in this country. These furnaces were later used in work by C.
Sykes on the properties of zirconium alloyed with various common metals.
Investigations
into the creep of metals were set in motion by R. W. Bailey about
1925 and have contributed much to the design of present-day power
plant, which requires alloys that will withstand temperatures far
above those used a few years ago. For instance, the work led to
the introduction of chromium-molybdenum bolt steel and of molybdenum-vanadium
steel for important parts of gas and steam turbines, including steam
piping. The latter alloy, familiar to the Company for more than
ten years, is now becoming generally recognized here and in America
as the only type of ferritic steel that can be used with the highest
steam temperatures and pressures in combination.
Later
studies, chiefly by A. M. Roberts, with a form of temperature-controlled
creep-tensile testing machine enabled the first batch of creep-testing
units to be designed. These have been in use since 1928, and the
extensive study of creep in the following years has been vital to
the development of jet engines and gas turbines.
In
1925 a six-element recording electromagnetic oscillograph was constructed
and installed, complete with dark room, near the main test beds
in the works, forming the nucleus of the present oscillographic
section. This is only one of the many pieces of testing apparatus
that have been developed in the research department for works use.
Examples are apparatus for the measurement of air flow in large
turbogenerators, resistance test sets, short-circuit coil testing
sets, iron loss test sets, temperature indicators for transformer
windings, an harmonic analyser for direct measurement on electrical
machines, and a.c. bridges for power measurement.
In
1926 came the brilliant discovery by C. R. Burch of the low-vapour
pressure oils and greases known as Apiezon compounds. Distillation
was a process that had always interested him, so it was natural
that the sight of a tank of 'steaming' transformer oil, the degassing
of which he had been asked to investigate, should reawaken the desire
to work on distillation—this time, on vacuum distillation.
"No chemist", he had been cynical enough to say, "knows
how to make a vacuum, and no vacuum worker has been interested in
distillation except Hevesy, and he has not applied molecular distillation
to organic chemistry. It would be rather jolly to distil mineral
oil under really high vacuum, in fact the best vacuum possible".
In this spirit Burch devised a molecular still and obtained distillates
having extremely low vapour pressures and therefore capable of being
used for high vacuum impregnation. Thus encouraged he developed
larger experimental stills incorporating the principles of molecular
distillation; an early commercial application was the concentration
and separation of vitamins in fish liver oils, where the high temperatures
normally required would have destroyed the vitamin content.
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